REACTION OF URACIL NUCLEOSIDES WITH 1-METHYLIMIDAZOLE IN THE PRESENCE OF PHOSPHORYL CHLORIDE: A CONVENIENT METHOD FOR THE SYNTHESIS OF 4-SUBSTITUED PYRIMIDIN-2(1H)-ONE NUCLEOSIDES
Reaction of 2',3',5'-tri-O-benzoyluridine (3) with 1-methylimidazole in the presence of phosphoryl chloride in acetonitrile afforded 3-methyl-1-imidazolium intermediate (4), from which a variety of 4-substituted pyrimidin-2(1H)-one ribosides (5-12) were o
Matsuda, Akira,Obi, Kikoh,Miyasaka, Tadashi
p. 2574 - 2578
(2007/10/02)
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