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Cas Database |
| Name |
Cyclopenta[c]pyrrole-1-carboxylic acid, octahydro-, ethyl ester, (1S,3aR,6aS)- |
EINECS | N/A |
| CAS No. | 1147103-42-1 | Density | N/A |
| PSA | 38.33000 | LogP | 2.06840 |
| Solubility | N/A | Melting Point |
N/A |
| Formula | C10H17NO2.HCl | Boiling Point | N/A |
| Molecular Weight | 219.711 | Flash Point | N/A |
| Transport Information | N/A | Appearance | N/A |
| Safety | Risk Codes | N/A | |
| Molecular Structure |
|
Hazard Symbols | N/A |
| Synonyms |
(1S,3aR,6aS)-Octahydrocyclopenta[c]pyrrole-1-car; |
Article Data | 2 |
Cyclopenta[c]pyrrole-1-carboxylic acid, octahydro-, ethyl ester, (1S,3aR,6aS)- Synthetic route
- 597569-42-1
(1S,3aR,6aS)-2-(tert-butoxycarbonyl)octahydrocyclo-penta[c]pyrrole-1-carboxylic acid
- 64-17-5
ethanol
- 1147103-42-1
C10H17NO2*ClH
Conditions
| Conditions | Yield |
|---|---|
| With thionyl chloride for 2h; Reflux; | 71% |
- 1053232-60-2
(1S,3aR,6aS)-hexahydro-cyclopenta[c]pyrrole-1,2-dicarboxylic acid 2-tert-butyl ester ethyl ester
- 1147103-42-1
C10H17NO2*ClH
Conditions
| Conditions | Yield |
|---|---|
| With hydrogenchloride In ethyl acetate at 30 - 35℃; for 4h; Inert atmosphere; Cooling with ice; | 70% |
- 1147103-42-1
C10H17NO2*ClH
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 3 steps 1: ethyl acetate / 12 h / 20 °C 2: sodium hydrogen sulfate / tert-butyl methyl ether; water 3: thionyl chloride / 2 h / Reflux View Scheme |
- 1147103-42-1
C10H17NO2*ClH
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 7 steps 1: sodium hydrogensulfite / tert-butyl methyl ether; water / 2 h / 20 °C 2: 3 h / 10 °C / pH 9 3: hydrogenchloride / water; dichloromethane / 1 h 4: sodium hydroxide / dichloromethane / 10 - 20 °C / pH 8 5: ethyl acetate / 12 h / 20 °C 6: sodium hydrogen sulfate / tert-butyl methyl ether; water 7: thionyl chloride / 2 h / Reflux View Scheme |
- 112626-50-3
(3aR,6aS)-octahydrocyclopenta[c]pyrrole hydrochloride
- 1147103-42-1
C10H17NO2*ClH
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 8 steps 1: sodium hypochlorite solution / tert-butyl methyl ether / 2 h / 15 °C 2: sodium hydrogensulfite / tert-butyl methyl ether; water / 2 h / 20 °C 3: 3 h / 10 °C / pH 9 4: hydrogenchloride / water; dichloromethane / 1 h 5: sodium hydroxide / dichloromethane / 10 - 20 °C / pH 8 6: ethyl acetate / 12 h / 20 °C 7: sodium hydrogen sulfate / tert-butyl methyl ether; water 8: thionyl chloride / 2 h / Reflux View Scheme |
- 1147103-42-1
C10H17NO2*ClH
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 6 steps 1: 3 h / 10 °C / pH 9 2: hydrogenchloride / water; dichloromethane / 1 h 3: sodium hydroxide / dichloromethane / 10 - 20 °C / pH 8 4: ethyl acetate / 12 h / 20 °C 5: sodium hydrogen sulfate / tert-butyl methyl ether; water 6: thionyl chloride / 2 h / Reflux View Scheme |
- 1147103-42-1
C10H17NO2*ClH
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 5 steps 1: hydrogenchloride / water; dichloromethane / 1 h 2: sodium hydroxide / dichloromethane / 10 - 20 °C / pH 8 3: ethyl acetate / 12 h / 20 °C 4: sodium hydrogen sulfate / tert-butyl methyl ether; water 5: thionyl chloride / 2 h / Reflux View Scheme |
- 1147103-42-1
C10H17NO2*ClH
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 4 steps 1: sodium hydroxide / dichloromethane / 10 - 20 °C / pH 8 2: ethyl acetate / 12 h / 20 °C 3: sodium hydrogen sulfate / tert-butyl methyl ether; water 4: thionyl chloride / 2 h / Reflux View Scheme |
- 597569-42-1
(1S,3aR,6aS)-2-(tert-butoxycarbonyl)octahydrocyclo-penta[c]pyrrole-1-carboxylic acid
- 64-17-5
ethanol
- 1147103-42-1
(1S,3aR,6aS)-ethyl octahydrocyclopenta[c]pyrrole-1-carboxylate hydrochloride
Conditions
| Conditions | Yield |
|---|---|
| With thionyl chloride for 2h; Reflux; | 71% |
- 1053232-60-2
(1S,3aR,6aS)-hexahydro-cyclopenta[c]pyrrole-1,2-dicarboxylic acid 2-tert-butyl ester ethyl ester
- 1147103-42-1
(1S,3aR,6aS)-ethyl octahydrocyclopenta[c]pyrrole-1-carboxylate hydrochloride
Conditions
| Conditions | Yield |
|---|---|
| With hydrogenchloride In ethyl acetate at 30 - 35℃; for 4h; Inert atmosphere; Cooling with ice; | 70% |
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(1S,3aR,6aS)-Octahydrocyclopenta[c]pyrrole-1-carboxylic acid ethyl ester hydrochloride
