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Cas Database |
| Name |
Dicyclohexylchlorophosphine |
EINECS | N/A |
| CAS No. | 16523-54-9 | Density | 1.054g/mLat 25°C(lit.) |
| PSA | 13.59000 | LogP | 5.28750 |
| Solubility | reacts violently with water | Melting Point |
126-128 °C |
| Formula | C12H22ClP | Boiling Point | 297.5 °C at 760 mmHg |
| Molecular Weight | 232.733 | Flash Point | 133.7 °C |
| Transport Information | UN 3265 8/PG 2 | Appearance | clear colorless liquid |
| Safety | 26-27-36/37/39-45-8 | Risk Codes | 14-34 |
| Molecular Structure |
|
Hazard Symbols |
 C
|
| Synonyms |
Phosphinouschloride, dicyclohexyl- (6CI,7CI,8CI,9CI);Chlorodicyclohexylphosphine;Dicyclohexylphosphinous chloride; |
Article Data | 15 |
Dicyclohexylchlorophosphine Synthetic route
- 829-84-5
dicyclohexylphosphane
- 16523-54-9
chlorodicyclohexylphosphane
| Conditions | Yield |
|---|---|
| With Ethyl trichloroacetate In chlorobenzene at 80℃; for 2.46667h; Product distribution / selectivity; | 80.6% |
- 931-51-1
cyclohexylmagnesiumchloride
- 16523-54-9
chlorodicyclohexylphosphane
| Conditions | Yield |
|---|---|
| With phosphorus trichloride | |
| With phosphorus trichloride In diethyl ether | |
| With phosphorus trichloride In toluene at 0℃; |
- 931-51-1
cyclohexylmagnesiumchloride
- 2844-89-5
dichlorocyclohexylphosphine
- 16523-54-9
chlorodicyclohexylphosphane
| Conditions | Yield |
|---|---|
| Irradiation; |
- 16523-54-9
chlorodicyclohexylphosphane
| Conditions | Yield |
|---|---|
| In chloroform at 20℃; |
- 16523-54-9
chlorodicyclohexylphosphane
| Conditions | Yield |
|---|---|
| In chloroform at 20℃; |
- 16523-54-9
chlorodicyclohexylphosphane
| Conditions | Yield |
|---|---|
| In chloroform at 20℃; |
- 108-85-0
1-bromocyclohexane
- 16523-54-9
chlorodicyclohexylphosphane
| Conditions | Yield |
|---|---|
| Stage #1: 1-bromocyclohexane With magnesium In tetrahydrofuran at 20℃; for 2h; Grignard reaction; Stage #2: With diethylphosphoramidous dichloride In tetrahydrofuran at 0 - 50℃; for 3h; phosphorylation; Stage #3: With hydrogenchloride In pentane at 0℃; for 1h; Hydrolysis; |
- 542-18-7
cyclohexyl chloride
- 16523-54-9
chlorodicyclohexylphosphane
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: Mg / diethyl ether / 2.5 h / Heating 2: PCl3 / diethyl ether View Scheme | |
| Stage #1: cyclohexyl chloride With magnesium In diethyl ether Stage #2: With phosphorus trichloride In diethyl ether at -40 - 20℃; for 5.33333h; | |
| Multi-step reaction with 2 steps 1: diethyl ether 2: phosphorus trichloride / diethyl ether / -40 - 20 °C View Scheme | |
| Stage #1: cyclohexyl chloride With magnesium In diethyl ether Stage #2: With phosphorus trichloride In tetrahydrofuran; diethyl ether at -40 - 20℃; for 7h; | |
| Multi-step reaction with 2 steps 1: magnesium / diethyl ether 2: phosphorus trichloride / tetrahydrofuran / 7 h / -40 - 20 °C View Scheme |
- 104202-80-4
trimethylsilyldicyclohexylphosphane
- 16523-54-9
chlorodicyclohexylphosphane
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: 100 percent / diethyl ether / -25 °C 2: CHCl3 / 20 °C View Scheme | |
| Multi-step reaction with 2 steps 1: 100 percent / diethyl ether / -25 °C 2: CHCl3 / 20 °C View Scheme | |
| Multi-step reaction with 2 steps 1: 100 percent / diethyl ether / -25 °C 2: CHCl3 / 20 °C View Scheme |
Dicyclohexylchlorophosphine Chemical Properties
Chemical Name: Dicyclohexylchlorophosphine
CAS No.: 16523-54-9
Molecular Formula: C12H22ClP
Formula Weight: 232.73 g/mol
Density: 1.054 g/mL at 25 °C(lit.)
Flash Point: 133.7 °C
Boiling Point: 297.5 °C at 760 mmHg
Sensitive: Air & Moisture Sensitive
Following is the structure of Dicyclohexylchlorophosphine (16523-54-9):
Product Categories about Dicyclohexylchlorophosphine (16523-54-9) are Chlorophosphines ; Phosphines ; Catalysis and Inorganic Chemistry ; Phosphorus Compounds ; Phosphorus Precursors
The chemical synonymous of Dicyclohexylchlorophosphine (16523-54-9) are Chlorodicyclohexylphosphine ; Dicyclohexylphosphinous chloride ; Dicyclohexylchlorophosphine ; Dicyclohexylchlorophosphine, 98+% ; Chlorodicyclohexylphosphine,97%
Dicyclohexylchlorophosphine Safety Profile
Hazard Codes:
C: Corrosive .gif){kind=small}
Risk Statements about Dicyclohexylchlorophosphine (16523-54-9):
R14 Reacts violently with water.
R34 Causes burns.
Safety Statements about Dicyclohexylchlorophosphine (16523-54-9):
S8 Keep container dry.
S26 In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
S36/37/39 Wear suitable protective clothing, gloves and eye/face protection.
Attentions:
1. Storage: Store in a cool, dry place. Store in a tightly closed container.
2. Handling: Do not breathe dust, vapor, mist, or gas. Do not get in eyes, on skin, or on clothing. Use only in a chemical fume hood. Handle under argon.
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