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Cas Database |
| Name |
Dimethyl azodiformate |
EINECS | N/A |
| CAS No. | 2446-84-6 | Density | 1.3g/cm3 |
| PSA | 77.32000 | LogP | 0.97140 |
| Solubility | N/A | Melting Point |
10°C |
| Formula | C4H6 N2 O4 | Boiling Point | 206.4°Cat760mmHg |
| Molecular Weight | 146.103 | Flash Point | 96.1°C |
| Transport Information | N/A | Appearance | N/A |
| Safety | A shock-sensitive explosive. It burns explosively when ignited. When heated to decomposition it emits toxic fumes of NOx. | Risk Codes | 11-36/37/38 |
| Molecular Structure |
|
Hazard Symbols | N/A |
| Synonyms |
Diazenedicarboxylicacid, dimethyl ester (9CI); Formic acid, azodi-, dimethyl ester (6CI,7CI,8CI);Azodicarboxylic acid, dimethyl ester; Dimethyl azodicarboxylate; Dimethylazodiformate; Dimethyl diazenedicarboxylate; NSC 522488 |
Article Data | 11 |
Dimethyl azodiformate Synthetic route
| Conditions | Yield |
|---|---|
| With dipotassium hydrogenphosphate for 1h; Reflux; | 98% |
- 135299-67-1
C7H15N3O6Si
- 2446-84-6
dimethyl azodicarboxylate
| Conditions | Yield |
|---|---|
| In dichloromethane at 25℃; for 72h; | 75% |
- 17643-54-8
N,N'-Bis-(methoxycarbonyl)-hydrazin
- 2446-84-6
dimethyl azodicarboxylate
| Conditions | Yield |
|---|---|
| With nitric acid |
- 1516-56-9
azidoformiate de methyle
A
- 50-00-0
formaldehyd
B
- 75-13-8
isocyanic acid
C
- 2446-84-6
dimethyl azodicarboxylate
D
- 117775-56-1
methoxy isocyanate
| Conditions | Yield |
|---|---|
| Irradiation; |
- 1516-56-9
azidoformiate de methyle
A
- 50-00-0
formaldehyd
B
- 75-13-8
isocyanic acid
C
- 2053-29-4
methyleneamine
D
- 2446-84-6
dimethyl azodicarboxylate
E
- 117775-56-1
methoxy isocyanate
| Conditions | Yield |
|---|---|
| Product distribution; Heating; further temp., pressure, residence time; |
- 946832-61-7
4,2',3'-trimethyl-4'-(p-fluorobenzyl)purpurogallin
- 2446-84-6
dimethyl azodicarboxylate
| Conditions | Yield |
|---|---|
| In toluene Heating; | 100% |
- 1002736-86-8
2-(p-fluorobenzyloxy)tropone
- 2446-84-6
dimethyl azodicarboxylate
| Conditions | Yield |
|---|---|
| In toluene hetero-Diels Alder reaction; Heating; | 100% |
- 1002736-87-9
2-(o-fluorobenzyloxy)tropone
- 2446-84-6
dimethyl azodicarboxylate
| Conditions | Yield |
|---|---|
| In toluene hetero-Diels Alder reaction; Heating; | 100% |
- 2446-84-6
dimethyl azodicarboxylate
- 153620-13-4
1,3-Bis-(1-cyclopenta-2,4-dienylidene-2,2-dimethyl-propyl)-benzene
- 153620-14-5
C34H42N4O8
| Conditions | Yield |
|---|---|
| In dichloromethane for 1h; | 99% |
Dimethyl azodiformate Chemical Properties
IUPAC Name: Methyl N-methoxycarbonyliminocarbamate
Synonyms of Dimethyl azodiformate (CAS NO.2446-84-6): Methyl azodicarboxylate ; Azodiformic acid dimethyl ester ; Azodicarboxylic acid dimethyl ester ; Dimethyl diazenedicarboxylate ; Dimethyl azodicarboxylate ; Azodicarboxylic acid dimethyl ester (40% in toluene) ; Dimethyl azodicarboxylate (40% in toluene, ca. 2.7mol/l) ; 1,2-Diazenedicarboxylic acid dimethyl ester ;
CAS NO: 2446-84-6
Molecular Formula of Dimethyl azodiformate (CAS NO.2446-84-6): C4H6N2O4
Molecular Weight: 146.1014
H bond acceptors: 6
H bond donors: 0
Freely Rotating Bonds: 4
Polar Surface Area: 77.32 Å2
Index of Refraction: 1.468
Molar Refractivity: 31.19 cm3
Molar Volume: 112 cm3
Surface Tension: 40.7 dyne/cm
Density: 1.3 g/cm3
Flash Point: 96.1 °C
Enthalpy of Vaporization: 44.26 kJ/mol
Boiling Point: 206.4 °C at 760 mmHg
Vapour Pressure: 0.238 mmHg at 25°C
Molecular Structure:
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Dimethyl azodiformate Safety Profile
Risk Statements of Dimethyl azodiformate (CAS NO.2446-84-6): 11-36/37/38
R11: Highly flammable. R36/37/38: Irritating to eyes, respiratory system and skin.
Safety Statements: 9-16-33
S9: Keep container in a well-ventilated place. S16: Keep away from sources of ignition. S33: Take precautionary measures against static discharges.
RIDADR: 1993
A shock-sensitive explosive. It burns explosively when ignited. When heated to decomposition it emits toxic fumes of NOx.
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