Heterocycles p. 217 - 225 (2007)
Update date:2022-09-26
Topics:
Majetich, George
Lift, Yang
Zou, Ge
(±)-Komaroviquinone (1) was synthesized from 3,4,5-trimethoxybenzoic acid in twenty-two steps. The key transformations in this synthesis are: (1) the construction of the cycloheptane ring via a Friedel-Crafts cyclialkylation; (2) a regiospecific benzylic oxidation; (3) a conformationally controlled introduction of the C(10) hydroxyl group and (4) intramolecular hemi-acetal formation.
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Doi:10.1016/j.tetasy.2007.12.016
(2008)Doi:10.1080/10426500701340949
(2007)Doi:10.1016/S0040-4020(02)00171-0
(2002)Doi:10.1021/ja078251w
(2008)Doi:10.1007/BF00515228
(1985)Doi:10.1021/jo702587e
(2008)