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(J¼272 Hz), 121.9, 115.6, 55.4, 28.0. MS (EI) m/z: 327 (Mþ1, 17), 326
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Acknowledgements
This research was supported by the University of the Basque
Country/Regional Government of Biscay/Basque Government
(Projects DIPE 06/10, UNESCO07/08 and GIU06/87/IT-349-07) and
the Spanish Ministry of Education and Science (MEC CTQ2007-
64501). The authors also thank S. A. Petronor for generous donation
of hexane.
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