Chemical Communications p. 11701 - 11703 (2016)
Update date:2022-08-03
Topics:
Thamm, Irene
Richers, Johannes
Rychlik, Michael
Tiefenbacher, Konrad
The short synthesis of α-thujone relies on the functionalization of the readily available dimethylfulvene. Furthermore, the three main metabolites of the natural product were also synthesized. Since d6-acetone can be used as a starting material, the route developed allows for the facile incorporation of isotopic labels which are required for detecting and quantifying trace amounts via GC/MS analysis.
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