Recueil des Travaux Chimiques des Pays-Bas p. 182 - 184 (1988)
Update date:2022-08-04
Topics:
Patel, Atula
Poller, Robert C.
N-Phthalation of 3-amino-3-deoxy-D-glucose was followed by replacement of the acidic proton by tributyl- and triphenylstannyl groups.A similar reaction with 1-(methylamino)-1-deoxy-D-glucitol failed and successive treatment with benzyl chloroformate and acetic anhydride followed by catalytic hydrogenation showed that a 1,4-O->N acetyl migration had occured.Phthalation and stannylation succeeded under different conditions.
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(1988)