Journal of Organic Chemistry p. 4791 - 4793 (1993)
Update date:2022-09-26
Topics:
Vidal, Joelle
Guy, Laure
Sterin, Sebastien
Collet, Andre
We describe the preparation of the title compound 2b via aza-Wittig reaction of N-Boc-triphenyliminophosphorane (6) with 4-cyanobenzaldehyde followed by Oxone oxidation of the resulting imine 5b.Oxaziridine 2b is a stable, crystalline solid, which transfers under mild conditions its N-Boc fragment to primary and secondary amines (to give Nβ-Boc-hydrazines) and enolates (to give N-Boc-amino drivatives).
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