Helvetica Chimica Acta p. 409 - 418 (1994)
Update date:2022-08-05
Topics:
Widhalm
Kalchhauser
Kahlig
The preparation of a macrocyclic diphosphine ligand 5 incorporating a binaphthyl unit and its Ni(II) and Pd(II) complexes, 6 and 7, is decribed. A complete assignment of 1H,- 13C-, and 31P-NMR data on the basis of 2D NMR spectroscopy (1H, 1H-, 13C, 1H-, 31P, 1H-, 31P, 13C-COSY) was possible for 5, and also - in part - for 6 and 7.
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