Journal of Organic Chemistry p. 4631 - 4633 (1981)
Update date:2022-08-02
Topics:
Hosomi, Akira
Shirahata, Akihiko
Araki, Yoshitaka
Sakurai, Hideki
α-Metalated imines, hydrazones, and activated methylene compounds are acetonylated with 3-chloro-2-(trimethylsiloxy)-1-propene in high yield.Highly regioselective acetonylation at either the tertiary or secondary α-carbon of 2-methylcyclohexanone can be carried out by selecting the reaction conditions.
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