Tetrahedron Asymmetry p. 1941 - 1946 (1995)
Update date:2022-08-03
Topics:
Nicoud
Cherkaoui
(S)-(-)-α,α-diphenyl-2-pyrrolidinemethanol reacts with 4-bromobenzenesulfinyl chloride to give a single diastereomer of the corresponding sulfinamide in high yield. By an acidic alcoholysis of the sulfinamide with primary alcohols one obtains enantiomerically pure new (R)-(+)-n-alkyl 4-bromobenzenesulfinates. The configurations of the sulfinamide and the sulfinates derived from it have been determined by 1H-NMR and molecular modeling.
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Doi:10.1039/DT9950003503
(1995)Doi:10.1248/cpb.46.1286
(1998)Doi:10.1016/0040-4039(95)01811-U
(1995)Doi:10.1016/00404-0399(50)1366-P
(1995)Doi:10.1021/jo00125a060
(1995)Doi:10.1002/chem.200800704
(2008)