Journal of Organometallic Chemistry p. 221 - 228 (1996)
Update date:2022-08-03
Topics:
Herzog
Richter
Brendler
Roewer
The methylchlorodisilanes SiCl2Me-SiCl2Me (1), SiCl2Me-SiClMe2 (2) and SiClMe2-SiClMe2 (3) disproportionate in the presence of a basic catalyst into methylchloromonosilanes and various methylchlorooligosilanes. Oligosilanes involving up to seven silicon atoms were identified by means of 29Si-, 13C-1H-NMR and GC-MS measurements. Formation of methylchlorooligosilanes is thought to take place via silylene intermediates.
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(1996)