Tetrahedron Letters p. 7649 - 7652 (1996)
Update date:2022-08-03
Topics:
Svensson, Anette
Fex, Tomas
Kihlberg, Jan
Gel-phase 19F NMR spectroscopy has been used to characterize products from a variety of reactions of fluorinated aromatics linked to a TentaGel resin. High quality spectra were obtained in a few minutes using an ordinary NMR spectometer, and the 19F chemical shifts of the support-bound compounds closely matched those of soluble references. In addition, substantial chemical shift differences were obtained for almost all of the synthetic transformations, illustrating the potential of 19F NMR for rapid monitoring of reactions in solid-phase organic synthesis.
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Doi:10.1016/0040-4039(96)01862-X
(1996)Doi:10.1016/0277-5387(96)00292-6
(1997)Doi:10.1021/ja962681x
(1996)Doi:10.1039/c9ra10663d
(2020)Doi:10.1021/ja9624331
(1996)Doi:10.1039/j39670002650
(1967)