Tetrahedron Letters p. 8969 - 8972 (1997)
Update date:2022-08-02
Topics:
Hashimoto, Shun-Ichi
Sakamoto, Hiroki
Honda, Takeshi
Abe, Hiroshi
Nakamura, Sei-Ichi
Ikegami, Shiro
A stereocontrolled synthesis of globotriaosylceramide with three different glycosidic linkages has been accomplished by linear and convergent routes exploiting 'armed-disarmed' glycosidation methodology based on glycosyl donors and acceptors carrying tetramethylphosphoroamidate as a leaving group. In particular, the convergent strategy featuring a coupling of a galactosyl(1→4)-galactosyl donor with a glucosylceramide derivative has proven to be extremely efficient.
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