Synthetic Communications p. 689 - 704 (2004)
Update date:2022-08-05
Topics:
Zheng, Qi-Huang
Wang, Ji-Quan
Liu, Xuan
Fei, Xiangshu
Mock, Bruce H.
Glick-Wilson, Barbara E.
Sullivan, Michael L.
Raikwar, Sudhanshu P.
Gardner, Thomas A.
Kao, Chinghai
Hutchins, Gary D.
An improved total synthesis of [18F]FHBG starting from triethyl-1,1,2-ethanetricarboxylate and 2-amino-6-chloropurine is reported. [18F]FHBG was prepared by nucleophilic substitution of the appropriate precursor with [18F]KF/Kryptofix 2.2.2 followed by a quick deprotection reaction and purification with a simplified Silica Sep-Pak solid-phase extraction (SPE) method in 20-25% radiochemical yield.
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