Tetrahedron Letters p. 5667 - 5670 (1999)
Update date:2022-08-03
Topics:
Roever, Stephan
Wipf, Peter
Fluorous alkoxysilyl protecting groups have been developed and evaluated for their acid stability. tert-Butylphenyl-1H,1H,2H,2H-heptadecafluorodecyloxysilyl (BPFOS) ethers in particular were found to be surprisingly acid stable and allow simple protection-purification-deprotection schemes by liquid-liquid extraction with FC-72/CH3CN or by solid phase extraction with fluorous reverse phase silica gel.
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Doi:10.1002/cctc.201901351
(2019)Doi:10.1021/jo9908849
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(2000)