Journal of the Chinese Chemical Society p. 601 - 605 (1999)
Update date:2022-08-05
Topics:
Ong, Chi Wi
Yen, Sin Fei
Chou, Yi Meen
The reaction of mercaptoacetaldehyde dialkyl acetals 1a-c in the presence of sulfuric acid, polyphosphoric acid and zinc chloride is described. Other than the disulfide reported previously, new compounds 1,2-bis-(mercapto)ethylene, 1,2,3-tris-(mercapto)ethane and 1,2-bis-(mercapto)methane have been isolated for the first time.
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Doi:10.1016/S0040-4039(00)01793-7
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