Tetrahedron Letters p. 8089 - 8092 (1998)
Update date:2022-09-26
Topics: Catalyst Alkyl halide Efficient preparation Finkelstein reaction E-β-iodovinyl phenylsulfone Vinylic center Metal halide salt
Zoller
Uguen
De Cian
Fischer
Treatment of E-β-chlorovinyl phenylsulfone, a crystalline compound that can be conveniently prepared on a large scale from 1,1,2-trichloroethane, by sodium iodide in acetone at ca 130 °C, in a sealed vessel, affords the title iodosulfone in good yield.
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