4392
J. I. 6an der Vlugt et al. / Tetrahedron Letters 44 (2003) 4389–4392
following dimensions: a=9.4589(1) A, b=0110.8619(2)
,
References
,
,
A, c=18.4500(3) A, h=80.1013(7)°, i=76.3222(6)°, k=
3
78.9500(10)°, V=1791.68(5) A , Dcalcd=1.221 g cm−3, 435
parameters, restraints, R(F)=0.0467 [I>2|(I)],
wR(F2)=0.1193, S=1.03, Dzmax/Dzmin=0.39/−0.34 e
,
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(
triclinic space group P1 (no. 2), Z=2 in cell with the