Journal of Organic Chemistry p. 6886 - 6894 (2019)
Update date:2022-08-03
Topics:
Salihila, Jonida
Silva, Lúcia
Pérez Del Pulgar, Helena
Quílez Molina, Ana
González-Coloma, Azucena
Olmeda, A. Sonia
Quílez Del Moral, José F.
Barrero, Alejandro F.
The system I2/dimethyl sulfoxide mediates the one-step transformation of α-isopropylidene ketones into furan rings following a biomimetic approach. This methodology has been used for the synthesis of terpene furans such as mintfurane, curzerene, atractylon, and isoatractylon, all of them possessing interesting biological activities. The synthesis of linderazulene directly from 4,5-epoxygermacrone via a cascade reaction shows the potential of this protocol. Additionally, this compound proved to show significant ixodicidal activity.
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