Tetrahedron p. 651 - 654 (1980)
Update date:2022-09-26
Topics:
Bokel, H. H.
Hoppmann, A.
Weyerstahl, P.
The dithiane 11 is alkylated with prenyl bromide to give 12.Hydrogenolysis of 12 with Raney-Nickel yields α-curcumene (6), hydrolysis of 12 gives the ketone 13.Prenal dithiane (14) is alkylated with 8 to give 15. ar-Turmerone (16) is formed by hydrolysis of 15.Reaction of 15 with sodium in liquid ammonia leads to a mixture of α-curcumene (6) and β-curcumene (10).
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Doi:10.1002/jhet.5570170518
(1980)Doi:10.1016/S0022-328X(00)86670-X
(1980)Doi:10.1002/jhet.3172
(2018)Doi:10.1081/SCC-120039503
(2004)Doi:10.1248/cpb.28.1971
(1980)Doi:10.1021/acs.jmedchem.9b01290
(2019)