Journal of Organic Chemistry p. 1266 - 1272 (2017)
Update date:2022-08-04
Topics: Suzuki-Miyaura coupling N-heterocyclic carbene Nickel Half-sandwich complex Precatalyst Aryl Heteroaryl Halides Boronic acids
Ando, Shin
Matsunaga, Hirofumi
Ishizuka, Tadao
A nickel half-sandwich complex supported by our original NHC ligand was developed as a robust precatalyst for Suzuki-Miyaura cross-coupling. The addition of PPh3 was a crucial element in the suppression of side reactions and in accelerating the cross-coupling reaction. By employing the optimal conditions, aryl-aryl, heteroaryl-aryl, and heteroaryl-heteroaryl couplings were achieved.
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