10.1002/adsc.202001209
Advanced Synthesis & Catalysis
2 (0.6 mmol, 1.2 equiv.) were added in one portion. The
Schlenk vessel was placed in a preheated oil bath (110–
120 °C) and the mixture was stirred for 30–42 h. The
reaction mixture was cooled to 23 °C and vented carefully.
After removal of all volatiles in vacuo the crude mixture was
purified by column chromatography on silica gel to afford
the desired products.
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Acknowledgements
X. Liu is grateful for the financial support of the Chinese
Scholarship Council (CSC). The authors gratefully acknowledge
the support from the LeibnizScience Campus Phosphorus
thanks Dr. Wu Li and Dr. Weiping Liu for their helpful suggestions.
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