Journal of the Chemical Society. Perkin transactions II p. 1301 - 1310 (1983)
Update date:2022-07-29
Topics:
Takeuchi, Ken'ichi
Murai, Osamu
Matsui, Shin
Inoue, Takeshi
Kitagawa, Toshikazu
Okamoto, Kunio
1,2,2,2-Tetrakis-(p-methoxyphenyl)ethanone (anispinacolone) (1) is cleaved by dibenzoyl peroxide (2) or bis-(3,5-dinitrobenzoyl) peroxide (3), affording tris-(p-methoxyphenyl)methyl benzoate (or 3,5-dinitrobenzoate) and benzoic (or 3,5-dinitrobenzoic) p-methoxybenzoic anhydride as the principal cleavage products. 13C N.m.r.CIDNP studies by use of labelled anispinacolone (An3*C-*COAn ; *C 90percent 13C) indicated that p-methoxybenzoyl radical is formed, presumably by way of the radical cation
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Doi:10.1007/BF00516459
(1983)Doi:10.3987/COM-05-S(K)58
(2005)Doi:10.1021/ja057257n
(2006)Doi:10.1016/S0040-4039(00)85969-9
(1983)Doi:10.1016/j.tetlet.2006.01.036
(2006)Doi:10.1246/cl.2006.172
(2006)