Phosphorus, Sulfur and Silicon and the Related Elements p. 1997 - 2003 (2006)
Update date:2022-07-29
Topics:
Nandeshwarappa, Belalakatte
Aruna Kumar, Doyijode
Bhojya Naik, Halehatty
Mahadevan, Kittappa
A convenient, efficient, and inexpensive procedure for the synthesis of 3-formyl-2-mercaptoquinolines 2a-l has been developed by a simple one-pot reaction of 3-formyl-2-chloroquinolines 1a-l with sodium sulfide and hydrochloric acid in ethanol. The structures of all the synthesized compounds were elucidated on the basis of elemental analyses and IR, 1 H NMR, and mass spectral data. Copyright Taylor & Francis Group, LLC.
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