Chemistry Letters p. 1765 - 1768 (1984)
Update date:2022-08-04
Topics:
Hiyama, Tamejiro
Nishide, Kiyoharu
Obayashi, Michio
An improved procedure for the preparation of trifluorovinylsilanes was established which involved addition of butyllithium to a mixture of chlorosilanes and commercially readily available chlorotrifluoroethylene at -78 to -130 deg C, and the resulting monomer was polymerized with a catalyst such as CsF or (R2N)3S(1+)*F2SiMe3(1-) to give black metallic polymer which showed conductivity of 1E-9 to 1E-10 Ω-1cm-1.
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