Synthetic Communications p. 2769 - 2772 (1998)
Update date:2022-07-30
Topics:
He, Zheng-Jie
Liu, Ju-Xiang
Tang, Chu-Chi
A general procedure for synthesis of phosphoro(-no)chlorides, particularly unsymmetrical ones, has been developed. The method involves the dealkylation of O,O-dialkyl phosphoro(-no)thionates 1 with dimethylamine and the chlorination of O-alkyl ammonium phosphoro(-no)thioates 2 using phosphorus oxychloride as a chlorinating agent.
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