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Green Chemistry
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ARTICLE
Journal Name
Experimental
DOI: 10.1039/C8GC03605E
Commun.,2013, 49, 11620-11622; (f) Q. Yang, T. Xu and
General Procedure for the synthesis of acetals
Z. Yu, Org. Lett., 2014, 16, 6310-6313.
In a glass vial with a screw cap containing thioxanthene-9-one (10.6
mg, 0.05 mmol) in alcohol (2 mL), aldehyde (0.50 mmol) was
added. The vial was sealed with a screw cap and left stirring under
household bulb irradiation (2 x 80W household lamps) for 1.5 h. The
desired product was isolated either by solvent evaporation,
distillation or after purification by column chromatography.
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H. Maarse, Volatile Compounds I Foods and Beverages,
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Acknowledgements
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404515 A4404511 19950817; (d) R. A. Ugarte and T.
The authors gratefully acknowledge financial support through the
Latsis Foundation programme “EPISTHMONIKES MELETES 2015”
W. Hudnall, Green Chem., 2017,19, 1990-1998.
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(a) J.-Y. Qi, J.-X. Ji, C.-H. Yueng, H.-L. Kwong and A. S. C.
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to Prof. V. Constantinou from the Agricultural University of Athens
for access to the fluorescence spectrometer and Dr. Maroula
Kokotou for her assistance in acquiring HRMS data. I.T. would like to
thank the Hellenic Foundation for Research and Innovation (ΕΛΙΔΕΚ)
and N. F. N. would like to thank the State Scholarships Foundation
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(IKY) for financial support. Also, COST Action C-H Activation in
Organic Synthesis (CHAOS) CA15106 is acknowledged for helpful
discussions.
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