Journal of Organic Chemistry p. 5357 - 5360 (1991)
Update date:2022-08-22
Topics:
El Ali, Bassam
Alper, Howard
Secondary and tertiary allylic alcohols react with carbon monoxide in the presence of catalytic quantities of bis(dibenzylideneacetone)palladium (0) and 1,4-bis(diphenylphosphino)butane affording lactones in 45-92percent isolated yields. α,β-Unsaturated acids are formed by isomerization and carbonylation of primary allylic alcohols. 2-(5H)-Furanones were isolated in yields of 60-80percent when alkynols were employed as substrates for the cyclocarbonylation process.
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