Bulletin of the Chemical Society of Japan p. 3200 - 3202 (1992)
Update date:2022-08-18
Topics:
Inokuchi, Tsutomu
Sugimoto, Tatsuya
Kusumoto, Masahiko
Torii, Sigeru
The methanesulfonates of α-hydroxy esters were converted to the corresponding deoxygenated esters in 70-88percent yields by the indirect electrolysis with diphenyl diselenide as a recyclable reagent in a divided cell.This deoxygenation method may involve the formation of α-phenylselenoester by replacement of α-methylsulfonyloxy group with phenylselenide anion followed by capture of the α-phenylseleno group with phenylselenide anion.
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