Phosphorus, Sulfur and Silicon and the Related Elements p. 980 - 983 (2016)
Update date:2022-08-29
Topics:
Dong, Wei-Li
Cai, Wen-Xi
Wu, Rui
Li, Zheng-Ming
Zhao, Wei-Guang
Liu, Xing-Hai
Benzenethiol, as a reductive agent for the dehalogenation of various α-halocarbonyl compounds, is investigated in the K+/CH3CN system. The reaction affords the reduced compounds in high yields under mild reaction conditions, especially α-chlorocarbonyl compounds. Furthermore, the reaction performed under ultrasonic irradiation greatly shortens the reaction time.
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