O.N. Shishilov et al. / Journal of Organometallic Chemistry 696 (2011) 2023e2029
2029
again. The crystals were obtained by storing the solution in a fridge
References
ꢁ
at 4 C during 2 weeks. The crystals were separated, washed with
0 ml of hexane and dried under vacuum. The yield is 10 mg
of crystals (4% based on Pd). Element analysis: found: C 31.69, H
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(CO)
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(
1.38%. IR-spectrum:
n
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n
(NO) 1624;
n
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ꢀ
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1516;
n
s
(CO
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(
[
[
(
4.7. X-ray crystallography
1
(
(
(
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(
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Appendix A. Supplementary data
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CCDC 772047, 772048 contain the supplementary crystallo-
graphic data for this paper. These data can be obtained free of
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