Chemistry Letters p. 2175 - 2178 (1994)
Update date:2022-08-30
Topics:
Kushi, Yoshinori
Nagao, Hirotaka
Nishioka, Takanori
Isobe, Kiyoshi
Tanaka, Koji
Electrochemical reduction of CO2 catalyzed by a triangular rhodium complex <(RhCp*)3(μ3-S)2>2+ selectively produced formate and oxalate in the presence of Bu4NBF4 and LiBF4, respectively, under the controlled potential electrolysis at -1.50 V (vs.SCE) in CO2-saturated CH3CN.A solution IR spectrum evidenced the adduct formation between <(RHCp*)3(μ3-S)2>0 and CO2 as the possible precursor for the oxalate formation.
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