Tetrahedron Letters p. 3051 - 3053 (2006)
Update date:2022-08-11
Topics:
Mahalingam
Wu, Xiongyu
Alterman, Mathias
Scandium triflate has been used as a convenient and efficient catalyst for removal of N-tert-butyl from amide groups. A variety of N-tert-butyl aryl and alkyl amides under these conditions gave the corresponding primary amide in high yields. With the use of microwave heating the deprotection reaction could be completed within 1 h.
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