Tetrahedron Letters p. 1179 - 1182 (1991)
Update date:2022-08-16
Topics:
Latouche, Regine
Texier-Boullet, Francoise
Hamelin, Jack
Condensation of trimethylsilylacetonitrile or ethyltrimethylsilylacetate with benzaldehyde, in the presence of dried alkali metal fluorides in heterogeneous media under microwaves leads readily to β-trimethylsilyloxynitrile or ester according to a Reformatsky type reaction.The later products could be hydrolyzed and dehydrated on the wet inorganic salt to give the corresponding alkenes.
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