Tetrahedron Letters p. 7219 - 7222 (1997)
Update date:2022-08-17
Topics:
Komatsu, Naoki
Ishida, Jun-Ya
Suzuki, Hitomi
The reductive homocoupling of carbonyl compounds and heterocoupling of a carbonyl compound with an alkoxysilane were both effected smoothly with triethylsilane in the presence of a catalytic amount of bismuth bromide (1-3 mol%) under mild conditions. This ether-forming reaction was successfully applied to the single-step preparation of novel crownophanes with olefinic or acetylenic linkages.
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