Synthetic Communications p. 361 - 367 (2007)
Update date:2022-08-22
Topics:
He, Wei
Zhang, Bang-Le
Zhou, Si-Yuan
Sun, Xiao-Li
Zhang, Sheng-Yong
Xanthotoxol, a biologically active linear furocoumarin, has been efficiently synthesized from 7-hydroxycoumarin in six steps. The key steps included two efficient rearrangements - Fries rearrangement and Claisen rearrangement - and a Baeyer-Villiger oxidation process. The overall yield of xanthotoxol was 29%. This approach also provided a new strategy to furnish easily furocoumarins with a hydroxyl group in the framework. Copyright Taylor & Francis Group, LLC.
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