Tetrahedron Letters p. 1669 - 1670 (1987)
Update date:2022-08-16
Topics:
Kim, Jin Hyung
Kim, Yong Hae
Various thiocarbonyl compounds such as thioamides, thiocarbamate, thiocarbonate, trithiocarbonate and thioketone were readily reacted with t-butyl thionitrate (t-BuSNO2) to give the corresponding carbonyl compounds in excellent yields under mild conditions.Desulfurization seems to be initiated via the selective nitrosation on the sulfur atom of thiocarbonyl group with t-BuSNO2.
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