Phosphorus, Sulfur and Silicon and the Related Elements p. 1727 - 1734 (2015)
Update date:2022-08-29
Topics:
Khalili, Dariush
Graphene oxide is described as a heterogeneous oxidant for the synthesis of symmetrical disulfides through the in situ generation of thiols from primary and secondary alkyl halides (tosylates) and thiourea in wet acetonitrile. A variety of alkyl halides and alkyl tosylates can be converted to corresponding disulfides in good to excellent yields. This strategy is free of foul-smelling thiols.
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