Chemistry of Heterocyclic Compounds p. 478 - 484 (2003)
Update date:2022-08-11
Topics:
Al-Subu
Jondi
Amer
Hannoun
Musmar
Reactions of morpholine, piperidine, and piperazine with Os(VIII) -catalyzed hexacyanoferrate(III) in alkaline media to produce the corresponding lactam have been studied at constant temperature and ionic strength. The reactions followed first-order kinetics with respect to [amine] and [Os(VIII)] but were independent of [Fe(CN)63-] and [OH-]. The effects of introduced electrolytes, potassium hexacyanoferrate(II), relative permitivity, and temperature have also been studied. A mechanism accounting for these results has been proposed.
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