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[15] Crystal data for 3: CCDC 819185, M=1765.15, Triclinic, P −1, a=14.607(3) Å,
(
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3
(
(3)°, V=4592.2(2) Å , Z=2, F(000)=1864,
R
1
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2
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2
3
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3
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(
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