Tetrahedron Letters p. 9361 - 9364 (2000)
Update date:2022-08-17
Topics:
Kanth
Brown
Diborane dissolves in chlorohydrocarbon solvents, such as dichloromethane, 1,2-dichloroethane and 1,1,2,2-tetrachloroethane to form ~0.5 M solutions of B2H6. In these solutions, diborane is in equilibrium with solvent-BH3 adducts (8-15%) and these solutions hydroborate representative olefins almost instantaneously, even at -16°C. The alcohol products can be obtained by standard oxidation of these organoboranes. (C) 2000 Elsevier Science Ltd.
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