Synthetic Communications p. 53 - 58 (1994)
Update date:2022-08-23
Topics:
Xie
Zhang
Yan
Yuan
Selective mono- and bis-oxidations of 2, 6-bis (hydroxy methyl) phenols with active M(n)O2 were realized, giving 2-hydroxy-3- hydroxymethyl benzaldehydes and 2-hydroxyisophthalaldehydes in good yields. The influence of oxidant activity, reaction solvent and temperature on the selectivity were investigated, and favorable conditions developed.
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