Bulletin of the Chemical Society of Japan p. 1767 - 1768 (1980)
Update date:2022-08-11
Topics:
Nakajima, Riichiro
Shintani, Yuji
Hara, Tadashi
Iodoarenes could be converted to the corresponding biaryls in high yields by use of a catalytic amount of a palladium amalgam in place of a palladium-calcium carbonate catalyst in Busch's reaction.The 2,3'-isomer content in the bitolyls obtained by the homo-coupling of o-iodotoluene was 15percent when palladium was used, while it was 1percent when a palladium amalgam was used, and the latter was re-usable.The present method is further applicable to some iodoalkanes.
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