Bulletin of the Academy of Sciences of the USSR Division of Chemical Science p. 561 - 566 (1991)
Update date:2022-08-11
Topics:
Ogibin, Yu. N.
Sokolov, A. B.
Ilovaiskii, A. I.
Elison, M. N.
Nikishin, G. I.
A study has been made of the electrochemical cleavage of the double bond of propenylbenzene (Ia) and p-propenylanisole (Ib), which takes place upon anodic oxidation of (Ia, b) in alcoholic solutions of sodium trifluoroacetate and other electrolytes and which leads to conversion of (Ia, b) to benzaldehyde dialkylacetals.Conditions are found that provide for highly selective (>80percent) conversion of (Ib) and p-propenyltoluene to p-methyl- and p-methoxybenzaldehyde dimethylacetals.
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