Tetrahedron p. 9823 - 9836 (1998)
Update date:2022-08-11
Topics:
Macdonald, Gregor
Alcaraz, Lilian
Wei, Xudong
Lewis, Norman J.
Taylor, Richard J. K.
A Stille palladium catalysed vinyl halide-vinyl stannane or aryl stannane coupling approach to the title compounds is described. The 2- aminocyclopentanedione-derived vinyl bromides (12, n = 1, 2, 3) were prepared and coupled to synthesise 2880-II (4), a Streptomyces metabolite, asuka-mABA (6), obtained during investigations to elucidate the biogenesis of the antibiotic asukamycin, and limocrocin (10), a naturally occurring antibiotic and antiviral agent.
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