Synthetic Communications p. 2378 - 2385 (2015)
Update date:2022-08-29
Topics:
Gao, Min
Lou, Chunqing
Zhu, Ning
Qin, Weijing
Suo, Quanling
Han, Limin
Hong, Hailong
A mild and practical method for the synthesis of 2-mercaptobenzothiazole has been developed by using iron as an efficient catalyst. The present tandem reaction process allows access to a wide range of 2-mercaptobenzothiazoles in good to excellent yields by the reaction of 2-haloaniline with potassium O-ethyl dithiocarbonate in the presence of FeF3 as a catalyst and 2,2′-bis(diphenylphosphino)-1,1′-binaphthyl as a ligand under an atmosphere of argon.
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