Journal of Organic Chemistry p. 5167 - 5175 (2015)
Update date:2022-08-10
Topics:
Satish, Gandhesiri
Polu, Ashok
Ramar, Thangeswaran
Ilangovan, Andivelu
(Chemical Equation Presented) Molecular iodine-promoted efficient construction of isatins from 2′-aminophenylacetylenes, 2′-aminostyrenes, and 2′-amino-β-ketoesters is developed via oxidative amidation of sp, sp2, and sp3 C-H bonds. The reaction involves consecutive iodination, Kornblum oxidation, and intramolecular amidation in a single reactor. The present method meets all of the atom and redox economy principles.
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