Russian Chemical Bulletin p. 640 - 644 (1996)
Update date:2022-08-10
Topics:
Ratner
Pashkevick
Fluoroalkyl-substituted allylic alcohols are readily and selectively oxidized at the hydroxyl group with the Swern or Dess-Martin reagents to give α,β-unsaturated ketones, and on treatment with m-chloroperbenzoic acid or tert-butyl hydroperoxide they are oxidized to the corresponding epoxyalcohols. The latter are oxidized by Swern or Dess-Martin reagents at the hydroxyl group to α,β-epoxyketones, which form hydrates stable under the conditions of isolation.
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